[2-(Me₂NCH₂)C₆H₄]PhSbCl

Base Information

• Chemical Name: [2-(Me₂NCH₂)C₆H₄]PhSbCl
• CAS No.: 1242187-81-0
• Molecular Formula: C₁₅H₁₇ClNSb
• Molecular Weight: 368.51

Synonyms:[2-(Me₂NCH₂)C₆H₄]PhSbCl

Chemical Property of [2-(Me₂NCH₂)C₆H₄]PhSbCl

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Technology Process of [2-(Me₂NCH₂)C₆H₄]PhSbCl

There total 1 articles about [2-(Me₂NCH₂)C₆H₄]PhSbCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

dichlorophenylstibine (5035-52-9) + 2-(N,N-dimethylaminomethyl)phenyllithium (56174-66-4) → [2-(Me2NCH2)C6H4]PhSbCl (1242187-81-0)

Guidance literature:

In hexane; (Ar, Schlenk technique); addn. of 1 equiv. of lithium compd. in hexane to hexane soln. of antimony compd. at -78°C, stirring for 2 h at -78°C, warming to room temp., stirring for 72 h; evapn., extn. (benzene), filtration, evapn., elem. anal.;

DOI:10.1039/c003318a

Reference yield: 97.0%

[2-(Me2NCH2)C6H4]PhSbCl (1242187-81-0) + potassium iodide (7681-11-0) → SbI(2-(dimethylamino)phenyl)(phenyl) (1242187-86-5)

Guidance literature:

In acetone; (Ar, Schlenk technique); stirring mixt. of KI and antimony compd. at room temp. for 12 h; filtration, evapn., elem. anal.;

DOI:10.1039/c003318a

Reference yield: 94.0%

dichloro bis(acetonitrile) palladium(II) (21264-30-2,90243-59-7,14592-56-4) + [2-(Me2NCH2)C6H4]PhSbCl (1242187-81-0) → C15H17Cl4NPdSb(1-)*C9H13N*H(1+)

Guidance literature:

In chloroform; acetonitrile; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c4ra03482a

upstream raw materials:

dichlorophenylstibine

2-(N,N-dimethylaminomethyl)phenyllithium

Downstream raw materials:

SbBr(2-(dimethylamino)phenyl)(phenyl)

SbI(2-(dimethylamino)phenyl)(phenyl)

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