7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester

Base Information

Chemical Name:7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester
CAS No.:140874-97-1
Molecular Formula:C₂₃H₂₉FO₃
Molecular Weight:372.48
Hs Code.:

Synonyms:7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester

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Chemical Property of 7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester

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Technology Process of 7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester

There total 1 articles about 7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 496-78-6
2,4,5-trimethylphenol

: 140875-12-3
7-(4-Fluoro-phenyl)-7-hydroxy-heptanoic acid methyl ester

: 140874-97-1
7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 60 ℃; for 6h;
DOI:10.1021/jm00090a009

Reference yield:

: 4885-02-3
Dichloromethyl methyl ether

: 140874-97-1
7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester

: 121099-95-4
7-(4-Fluoro-phenyl)-7-(4-formyl-2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester

Guidance literature:: With titanium tetrachloride; In 1,2-dichloro-ethane; at -12 - -10 ℃; for 0.333333h;
DOI:10.1021/jm00090a009

Reference yield:

: 140874-97-1
7-(4-Fluoro-phenyl)-7-(2-hydroxy-3,5,6-trimethyl-phenyl)-heptanoic acid methyl ester

: 140874-91-5
7-(4-Fluoro-phenyl)-7-(2-hydroxy-4-hydroxymethyl-3,5,6-trimethyl-phenyl)-heptanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: TiCl₄ / 1,2-dichloro-ethane / 0.33 h / -12 - -10 °C

2: 47 percent / NaOH / methanol / 15 h / Ambient temperature

3: 64 percent / NaBH₄ / tetrahydrofuran / 2 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; titanium tetrachloride; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;
DOI:10.1021/jm00090a009