tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

Base Information

Chemical Name:tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)
CAS No.:116025-84-4
Molecular Formula:C₄₆H₅₁P₄Rh
Molecular Weight:830.711
Hs Code.:

Synonyms:tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

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Chemical Property of tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

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Technology Process of tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

There total 1 articles about tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 107197-98-8
[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

: 65567-06-8,4541-02-0
lithium diphenylphosphide

: 116025-84-4
tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

Guidance literature:: In diethyl ether; byproducts: LiCl; N2 atmosphere, slow warming (from -20°C to room temp.,), stirring (16 h); filtn., pptn. on hexane addn., drying (vacuum); elem. anal.;

Reference yield: 94.0%

: 116025-84-4
tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

: 116025-87-7
[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]dichlorohydridorhodium(III)

Guidance literature:: With HCl; In toluene; byproducts: HPPh2; N2 atmosphere, pptn.; washing (ether), drying (vacuum); elem. anal.;

Reference yield: 90.0%

: 116025-84-4
tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

: 116026-02-9
tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphine)(hydrido)rhodium(I)

Guidance literature:: With hydrogen; In toluene; N2 atmosphere, bubbling of H2, stirring (10-15 min, H2); concn., pptn. on hexane addn., washing (hexane), drying (vacuum); elem. anal.;