[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

Base Information

Chemical Name:[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)
CAS No.:107197-98-8
Molecular Formula:C₃₄H₄₁ClP₃Rh
Molecular Weight:680.979
Hs Code.:

Synonyms:[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

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Chemical Property of [tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

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Technology Process of [tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

There total 3 articles about [tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 116025-85-5
tert-butylbis(3-diphenylphosphinopropyl)phosphine(dicyclohexylphosphido)rhodium(I)

: 107197-98-8
[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

Guidance literature:: With methyl chloride; In toluene; byproducts: methyldicyclohexylphosphine; N2 atmosphere, room temp.; concn., pptn. on hexane addn.;

Reference yield: 74.0%

: 116025-84-4
tert-butylbis(3-diphenylphosphinopropyl)phosphine(diphenylphosphido)rhodium(I)

: 107197-98-8
[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

Guidance literature:: With methyl chloride; In toluene; byproducts: methyldiphenylphosphine; N2 atmosphere, room temp.; concn., pptn. on hexane addn.;

Reference yield:

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 107164-43-2
Bis(3-diphenylphosphanopropyl)tert.-butylphosphan

: 107197-98-8
[tert-butylbis(3-(diphenylphosphanyl)propyl)phosphane]chlororhodium(I)

Guidance literature:: In toluene; under inert gas atmosphere; stirring of a soln. of the Rh-compd. and the phosphane in toluene for 2 h at room temp.; pptd. crystals are filtered off, washed with hexane and dried in vac.; partial evapn. of solvent from mother liquor and pptn. with hexane yields further Rh-complex; elem. anal.;