2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Base Information

• Chemical Name: 2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine
• CAS No.: 153046-52-7
• Molecular Formula: C₄₈H₄₈N₃O₉P₃
• Molecular Weight: 903.845

Synonyms:2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Chemical Property of 2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

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Technology Process of 2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

There total 2 articles about 2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-trichloro-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (220976-07-8) + phenol (108-95-2,27073-41-2) → 2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (153046-52-7)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 24h; Heating;

DOI:10.1007/PL00010178

Reference yield:

4-allylguaiacol (97-53-0) → 2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (153046-52-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 10.1 g / hexachlorocyclotriphosphazene, NaH / tetrahydrofuran / 1) 20 deg C, 12 h, 2) reflux, 4 h

2: 71 percent / NaH / tetrahydrofuran / 24 h / Heating

With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; sodium hydride; In tetrahydrofuran;

DOI:10.1007/PL00010178

Reference yield: 78.0%

Triethoxysilane (998-30-1) + 2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-triphenoxy-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (153046-52-7) → C66H96N3O18P3Si3

Guidance literature:

dihydrogen hexachloroplatinate; In tetrahydrofuran; isopropyl alcohol; for 24h; Heating;

DOI:10.1007/PL00010178

upstream raw materials:

2,4,6-Tris-(4-allyl-2-methoxy-phenoxy)-2,4,6-trichloro-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

phenol

4-allylguaiacol

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