Technology Process of C15H11F3N4O
There total 4 articles about C15H11F3N4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hexamethyldisilazane;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one;
at 150 ℃;
for 1h;
Inert atmosphere;
Microwave irradiation;
DOI:10.1016/j.tetlet.2011.12.132
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap
2: ethanol / 0.5 h / 150 °C / Microwave irradiation
3: sodium hexamethyldisilazane / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 1 h / 150 °C / Inert atmosphere; Microwave irradiation
With
dmap; sodium hexamethyldisilazane;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol;
DOI:10.1016/j.tetlet.2011.12.132
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap
2: ethanol / 0.5 h / 150 °C / Microwave irradiation
3: sodium hexamethyldisilazane / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 1 h / 150 °C / Inert atmosphere; Microwave irradiation
With
dmap; sodium hexamethyldisilazane;
In
tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethanol;
DOI:10.1016/j.tetlet.2011.12.132