(1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine

Base Information

Chemical Name:(1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine
CAS No.:950829-02-4
Molecular Formula:C₂₈H₂₇NO₂S
Molecular Weight:441.594
Hs Code.:

Synonyms:(1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine

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Chemical Property of (1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine

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Technology Process of (1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine

There total 3 articles about (1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 10381-68-7,42872-16-2,78821-95-1,1517-78-8
(S)-2-methyl-1-(p-tolylsulfinyl)benzene

: 1613-90-7
4-methoxy-N-[(E)-phenylmethylidene]aniline

: 950829-01-3
(1S)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine

: 950829-02-4
(1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine

Guidance literature:: (S)-2-methyl-1-(p-tolylsulfinyl)benzene; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

4-methoxy-N-[(E)-phenylmethylidene]aniline; In tetrahydrofuran; hexane; at -78 ℃; Further stages.;
DOI:10.1002/chem.200601893

Reference yield:

: 100-52-7
benzaldehyde

: 950829-02-4
(1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / 4 Angstroem molecular sieves / CH₂Cl₂ / 20 °C

2.1: nBuLi; iPr₂NH / hexane; tetrahydrofuran / 0.25 h / -78 °C

2.2: 56 percent / hexane; tetrahydrofuran / -78 °C

With n-butyllithium; 4 A molecular sieve; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/chem.200601893

Reference yield:

: 104-94-9
4-methoxy-aniline

: 950829-02-4
(1R)-N-(4-methoxyphenyl)-1-phenyl-2-{2-[(S)-p-tolylsulfinyl]phenyl}ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / 4 Angstroem molecular sieves / CH₂Cl₂ / 20 °C

2.1: nBuLi; iPr₂NH / hexane; tetrahydrofuran / 0.25 h / -78 °C

2.2: 56 percent / hexane; tetrahydrofuran / -78 °C

With n-butyllithium; 4 A molecular sieve; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/chem.200601893