4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester

Base Information

Chemical Name:4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester
CAS No.:172364-40-8
Molecular Formula:C₂₃H₃₃NO₄Si
Molecular Weight:415.605
Hs Code.:

Synonyms:4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester

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Chemical Property of 4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester

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Technology Process of 4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester

There total 1 articles about 4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 4229-44-1
N-methylhydroxyamine hydrochloride

: 260445-02-1
(+/-)-ethyl trans-4-(tert-butyldiphenylsilyloxy)-2-butenoate

: 172364-40-8
4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1016/0040-4039(95)01499-8

Reference yield:

: 172364-40-8
4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester

: 4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butan-1-ol

: (R)-3-(tert-Butyl-diphenyl-silanyloxymethyl)-2-methyl-isoxazolidin-5-ol

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 ℃; for 1h; Title compound not separated from byproducts;
DOI:10.1016/0040-4039(95)01499-8

Reference yield:

: 75-36-5
acetyl chloride

: 172364-40-8
4-(tert-Butyl-diphenyl-silanyloxy)-3-(hydroxy-methyl-amino)-butyric acid ethyl ester

: C₂₃H₃₁NO₄Si

: C₂₅H₃₅NO₅Si

Guidance literature:: With diisobutylaluminium hydride; triethylamine; Yield given. Multistep reaction; 1.) PhMe, -78 deg C, 1 h; 2.) CH₂Cl₂, RT;
DOI:10.1016/0040-4039(95)01499-8