2-{[(Z)-(3-methoxy-4-oxocyclohexa-2,5-dien-1-ylidene)methyl]amino}-6,7-dihydro-1H-indeno[6,7,1-def]isoquinoline-1,3(2H)-dione

Base Information

Chemical Name:2-{[(Z)-(3-methoxy-4-oxocyclohexa-2,5-dien-1-ylidene)methyl]amino}-6,7-dihydro-1H-indeno[6,7,1-def]isoquinoline-1,3(2H)-dione
CAS No.:5737-78-0
Molecular Formula:C₁₄H₁₁NO₄
Molecular Weight:257.246
Hs Code.:

Synonyms:methyl 2'-nitro-[1,1'-biphenyl]-4-carboxylate

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Chemical Property of 2-{[(Z)-(3-methoxy-4-oxocyclohexa-2,5-dien-1-ylidene)methyl]amino}-6,7-dihydro-1H-indeno[6,7,1-def]isoquinoline-1,3(2H)-dione

Chemical Property:

Vapor Pressure:2.56E-16mmHg at 25°C

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Technology Process of 2-{[(Z)-(3-methoxy-4-oxocyclohexa-2,5-dien-1-ylidene)methyl]amino}-6,7-dihydro-1H-indeno[6,7,1-def]isoquinoline-1,3(2H)-dione

There total 1 articles about 2-{[(Z)-(3-methoxy-4-oxocyclohexa-2,5-dien-1-ylidene)methyl]amino}-6,7-dihydro-1H-indeno[6,7,1-def]isoquinoline-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 577-19-5
2-nitrophenyl bromide

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 5737-78-0
methyl 2'-nitro-[1,1'-biphenyl]-4-carboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; N,N-dimethyl-formamide; at 80 ℃; for 5h; Inert atmosphere;
DOI:10.1002/anie.201309973

Reference yield: 90.0%

: 5737-78-0
methyl 2'-nitro-[1,1'-biphenyl]-4-carboxylate

: 5737-79-1
methyl 2′-amino-[1,1′-biphenyl]-4-carboxylate

Guidance literature:: With iron; acetic acid; In water; acetone; for 4h; Reflux;
DOI:10.1016/j.tetlet.2020.152750

Reference yield: 85.0%

: 5737-78-0
methyl 2'-nitro-[1,1'-biphenyl]-4-carboxylate

: 26000-33-9
methyl 9H-carbazole-2-carboxylate

Guidance literature:: With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; triphenylphosphine; In 1,4-dioxane; at 55 ℃; for 72h; Inert atmosphere; Irradiation;
DOI:10.1016/j.cclet.2021.02.047