(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid

Base Information

Chemical Name:(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid
CAS No.:852332-12-8
Molecular Formula:C₂₉H₃₄N₂O₈
Molecular Weight:538.598
Hs Code.:

Synonyms:(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid

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Chemical Property of (1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid

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Technology Process of (1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid

There total 5 articles about (1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.4%

: 852332-11-7
(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester

: 852332-12-8
(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; dichloromethane; isopropyl alcohol; for 72h;
DOI:10.1002/chem.200500007

Reference yield:

: (1R,3S,5R)-5-(Imidazole-1-carbonyl)-cyclohexane-1,3-dicarboxylic acid

: 852332-12-8
(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 38.16 g / dimethylsulfoxide; ethyl acetate

2: 45 percent / Et₃N; DMT-MM / methanol / 20 °C

3: 97 percent / H₂ / Pd/C / methanol; propan-2-ol; CH₂Cl₂ / 72 h

With hydrogen; triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; palladium on activated charcoal; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; isopropyl alcohol;
DOI:10.1002/chem.200500007

Reference yield:

: 852332-10-6
CHex(OBn)(COOH)2

: 852332-12-8
(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / Et₃N; DMT-MM / methanol / 20 °C

2: 97 percent / H₂ / Pd/C / methanol; propan-2-ol; CH₂Cl₂ / 72 h

With hydrogen; triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; palladium on activated charcoal; In methanol; dichloromethane; isopropyl alcohol;
DOI:10.1002/chem.200500007