(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester

Base Information

Chemical Name:(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester
CAS No.:852332-11-7
Molecular Formula:C₃₆H₄₀N₂O₈
Molecular Weight:628.722
Hs Code.:

Synonyms:(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester

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Chemical Property of (1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester

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Technology Process of (1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester

There total 3 articles about (1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 852332-10-6
CHex(OBn)(COOH)2

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 852332-11-7
(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester

Guidance literature:: With triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In methanol; at 20 ℃;
DOI:10.1002/chem.200500007

Reference yield:

: (1R,3S,5R)-5-(Imidazole-1-carbonyl)-cyclohexane-1,3-dicarboxylic acid

: 852332-11-7
(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 38.16 g / dimethylsulfoxide; ethyl acetate

2: 45 percent / Et₃N; DMT-MM / methanol / 20 °C

With triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In methanol; dimethyl sulfoxide; ethyl acetate;
DOI:10.1002/chem.200500007

Reference yield:

: 16526-68-4
cis-1,3,5-cyclohexane tricarboxylic acid

: 852332-11-7
(1S,3R,5S)-3,5-Bis-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-cyclohexanecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfoxide; ethyl acetate / 2 h

2: 38.16 g / dimethylsulfoxide; ethyl acetate

3: 45 percent / Et₃N; DMT-MM / methanol / 20 °C

With triethylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In methanol; dimethyl sulfoxide; ethyl acetate;
DOI:10.1002/chem.200500007