(Z)-4-(bis(ethylthio)methylene)-5-((E)-3-(bis(ethylthio)methylene)-2,6-bis(4-chlorophenyl)-4-oxohex-5-enylidene)dihydrofuran-2,3-dione

Base Information

Chemical Name:(Z)-4-(bis(ethylthio)methylene)-5-((E)-3-(bis(ethylthio)methylene)-2,6-bis(4-chlorophenyl)-4-oxohex-5-enylidene)dihydrofuran-2,3-dione
CAS No.:1170697-88-7
Molecular Formula:C₃₂H₃₂Cl₂O₄S₄
Molecular Weight:679.774
Hs Code.:

Synonyms:(Z)-4-(bis(ethylthio)methylene)-5-((E)-3-(bis(ethylthio)methylene)-2,6-bis(4-chlorophenyl)-4-oxohex-5-enylidene)dihydrofuran-2,3-dione

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Chemical Property of (Z)-4-(bis(ethylthio)methylene)-5-((E)-3-(bis(ethylthio)methylene)-2,6-bis(4-chlorophenyl)-4-oxohex-5-enylidene)dihydrofuran-2,3-dione

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Technology Process of (Z)-4-(bis(ethylthio)methylene)-5-((E)-3-(bis(ethylthio)methylene)-2,6-bis(4-chlorophenyl)-4-oxohex-5-enylidene)dihydrofuran-2,3-dione

There total 1 articles about (Z)-4-(bis(ethylthio)methylene)-5-((E)-3-(bis(ethylthio)methylene)-2,6-bis(4-chlorophenyl)-4-oxohex-5-enylidene)dihydrofuran-2,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 79-37-8
oxalyl dichloride

: 874149-44-7
C₁₅H₁₇ClOS₂

: 1170697-88-7
(Z)-4-(bis(ethylthio)methylene)-5-((E)-3-(bis(ethylthio)methylene)-2,6-bis(4-chlorophenyl)-4-oxohex-5-enylidene)dihydrofuran-2,3-dione

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; stereospecific reaction;
DOI:10.1021/jo900764s

Reference yield:

: 1170697-88-7
(Z)-4-(bis(ethylthio)methylene)-5-((E)-3-(bis(ethylthio)methylene)-2,6-bis(4-chlorophenyl)-4-oxohex-5-enylidene)dihydrofuran-2,3-dione

: S-ethyl 2-(7-(bis(ethylthio)methylene)-6,9-bis(4-chlorophenyl)-2-(ethylthio)-4,8-dioxobicyclo[3.3.1]non-2-en-3-yl)-2-oxoethanethioate

: S-ethyl 2-(7-(bis(ethylthio)methylene)-6,9-bis(4-chlorophenyl)-2-(ethylthio)-4,8-dioxobicyclo[3.3.1]non-2-en-3-yl)-2-oxoethanethioate

Guidance literature:: With boron trifluoride diethyl etherate; In acetonitrile; at 20 ℃; for 7h; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/jo900764s