Technology Process of C41H54O8Si
There total 7 articles about C41H54O8Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap;
In
N,N-dimethyl-formamide;
at 25 ℃;
for 1h;
DOI:10.1021/ja00107a009
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu4NBH4
2: 76 percent / KH, n-Bu4NI / diethyl ether; hexamethylphosphoric acid triamide / 4 h / 25 °C
3: 98 percent / DBU / methanol; CH2Cl2 / 3 h / 25 °C
4: DMAP / dimethylformamide / 1 h / 25 °C
With
dmap; tetra-(n-butyl)ammonium iodide; potassium hydride; tetrabutylammonium borohydride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00107a009
- Guidance literature:
-
Multi-step reaction with 5 steps
1: p-toluenesulfonic acid / methanol / 48 h / 25 °C
2: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu4NBH4
3: 76 percent / KH, n-Bu4NI / diethyl ether; hexamethylphosphoric acid triamide / 4 h / 25 °C
4: 98 percent / DBU / methanol; CH2Cl2 / 3 h / 25 °C
5: DMAP / dimethylformamide / 1 h / 25 °C
With
dmap; tetra-(n-butyl)ammonium iodide; potassium hydride; tetrabutylammonium borohydride; Dess-Martin periodane; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00107a009
