(E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one

Base Information

Chemical Name:(E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one
CAS No.:1425861-26-2
Molecular Formula:C₃₅H₄₅NO₆
Molecular Weight:575.745
Hs Code.:

(E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one

Synonyms:(E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one

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Chemical Property of (E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one

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Technology Process of (E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one

There total 13 articles about (E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1425861-31-9
(4E)-1,1-diethoxy-3,7,11-trimethyldodeca-2,6,10-triene

: 1425861-04-6
4-hydroxy-6-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-2,3-dihydro-isoindol-1-one

: 1425861-26-2
(E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one

Guidance literature:: With 3-Methylpyridine; In o-xylene; for 48h; Reflux;
DOI:10.1055/s-0032-1317528

Reference yield:

: 29655-46-7
N-benzyloxycarbonyl-2-(4-hydroxyphenyl)ethylamine

: 1425861-26-2
(E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h

3.1: methanol / 1 h

3.2: 0 - 20 °C

4.1: 3-Methylpyridine / o-xylene / 48 h / Reflux

With 3-Methylpyridine; palladium 10% on activated carbon; hydrogen; sodium hydride; In methanol; o-xylene; N,N-dimethyl-formamide; mineral oil;
DOI:10.1055/s-0032-1317528

Reference yield:

: 99-10-5
3,5-Dihydroxybenzoic acid

: 1425861-26-2
(E)-8-(4,8-dimethylnona-3,7-dienyl)-5-methoxymethoxy-2-[2-(4-methoxymethoxyphenyl)ethyl]-8-methyl-1,2-dihydro-8H-9-oxa-2-azacyclopenta[a]naphthalen-3-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / 20 °C / Reflux

2.1: aluminum (III) chloride; hydrogenchloride / diethyl ether / 0 - 20 °C

3.1: potassium carbonate / acetone / 12 h / 20 °C

4.1: methanol / 1 h

4.2: 0 - 20 °C

5.1: 3-Methylpyridine / o-xylene / 48 h / Reflux

With hydrogenchloride; aluminum (III) chloride; thionyl chloride; 3-Methylpyridine; potassium carbonate; In methanol; diethyl ether; o-xylene; acetone;
DOI:10.1055/s-0032-1317528