cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride

Base Information

Chemical Name:cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride
CAS No.:125365-13-1
Molecular Formula:C₄₃H₄₄O₈
Molecular Weight:688.818
Hs Code.:

Synonyms:cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride

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Chemical Property of cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride

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Technology Process of cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride

There total 3 articles about cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 108-31-6
maleic anhydride

: 125365-10-8
5-(tetra-O-benzyl-α-D-glucopyranosyl)-(E)-1,3-pentadiene

: 125365-13-1
cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride

Guidance literature:: In toluene; at 80 - 90 ℃; for 8h;
DOI:10.1016/0008-6215(89)85066-9

Reference yield:

: 4196-36-5
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl 4-nitrobenzoate

: 125365-13-1
cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / BF₃*OEt₂ / acetonitrile / 0 °C

2: 78 percent / toluene / 8 h / 80 - 90 °C

With boron trifluoride diethyl etherate; In toluene; acetonitrile;
DOI:10.1016/0008-6215(89)85066-9

Reference yield:

: 72952-73-9
(E)-2,4-pentadienyltrimethylsilane

: 125365-13-1
cis-cis-3-(tetra-O-benzyl-α-D-glucopyranosylmethyl)cyclohex-4-ene-1,2-dicarboxylic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / BF₃*OEt₂ / acetonitrile / 0 °C

2: 78 percent / toluene / 8 h / 80 - 90 °C

With boron trifluoride diethyl etherate; In toluene; acetonitrile;
DOI:10.1016/0008-6215(89)85066-9