(S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate

Base Information

Chemical Name:(S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate
CAS No.:1352917-67-9
Molecular Formula:C₉H₁₀O₃*C₁₄H₂₁NO
Molecular Weight:385.503
Hs Code.:

Synonyms:(S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate

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Chemical Property of (S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate

Chemical Property:

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Technology Process of (S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate

There total 4 articles about (S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 20312-36-1
L-3-phenyllactic acid

: 78598-91-1,3899-07-8
2-(N-propylamino)-5-methoxytetraline

: 1352917-67-9
(S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate

Guidance literature:: In methyltretrahydrofuran, 2-; at 25 - 70 ℃; for 16.5h; Product distribution / selectivity;

Reference yield:

: 3904-24-3
(5-methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)propylamine hydrochloride

: 1352917-67-9
(S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / 2-methyltetrahydrofuran / Reflux

2: methyltretrahydrofuran, 2- / 16.5 h / 25 - 70 °C

With potassium carbonate; In 2-methyltetrahydrofuran; methyltretrahydrofuran, 2-;

Reference yield:

: 3880-88-4,58349-15-8,58349-17-0
SKF 87967 hydrochloride

: 1352917-67-9
(S)-1,2,3,4-tetrahydro-5-methoxy-N-propyl-naphthalen-2-ammonium (S)-2-hydroxy-3-phenylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium acetate; acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran / 0 - 10 °C

1.2: 0.5 h / 0 - 20 °C

1.3: 1.33 h / 10 - 50 °C

2.1: potassium carbonate / 2-methyltetrahydrofuran / Reflux

3.1: methyltretrahydrofuran, 2- / 16.5 h / 25 - 70 °C

With sodium acetate; sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; In tetrahydrofuran; 2-methyltetrahydrofuran; methyltretrahydrofuran, 2-;