N,N,N,3,5-pentamethylbenzenaminium iodide

Base Information

• Chemical Name: N,N,N,3,5-pentamethylbenzenaminium iodide
• CAS No.: 13330-20-6
• Molecular Formula: C₁₁H₁₈N*I
• Molecular Weight: 291.175
• Mol file: 13330-20-6.mol

Synonyms:N,N,N,3,5-pentamethylbenzenaminium iodide

Chemical Property of N,N,N,3,5-pentamethylbenzenaminium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N,N,3,5-pentamethylbenzenaminium iodide

There total 1 articles about N,N,N,3,5-pentamethylbenzenaminium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethylaminoaniline (108-69-0) + methyl iodide (74-88-4) → N,N,N,3,5-pentamethylbenzenaminium iodide (13330-20-6)

Guidance literature:

With water; sodium carbonate;

Reference yield: 90.0%

N,N,N,3,5-pentamethylbenzenaminium iodide (13330-20-6) + bis(pinacol)diborane (73183-34-3) → 2-(3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (325142-93-6)

Guidance literature:

With 10H-phenothiazine; caesium carbonate; In acetonitrile; for 18h; Wavelength; Irradiation; Sealed tube; Inert atmosphere;

DOI:10.1021/jacs.9b12519

Reference yield:

N,N,N,3,5-pentamethylbenzenaminium iodide (13330-20-6) → 3,5,N,N-tetramethylaniline (4913-13-7)

Guidance literature:

durch Ueberfuehren in die quartaere Base und Destillieren;

upstream raw materials:

3,5-dimethylaminoaniline

methyl iodide

Downstream raw materials:

3,5,N,N-tetramethylaniline

2-(3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane