3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

Base Information

Chemical Name:3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid
CAS No.:1381849-05-3
Molecular Formula:C₂₄H₂₈O₆
Molecular Weight:412.483
Hs Code.:

Synonyms:3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

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Chemical Property of 3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

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Technology Process of 3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

There total 3 articles about 3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1381849-04-2
benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

: 1381849-05-3
3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

Guidance literature:: benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate; With sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In water; acetonitrile; pH=2; Inert atmosphere;
DOI:10.1016/j.bmc.2012.04.034

Reference yield:

: 103-40-2
succinic acid monobenzyl ester

: 1381849-05-3
3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0 - 23 °C / Inert atmosphere

2.1: water; acetic acid / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / acetonitrile / 0 - 20 °C / Inert atmosphere

4.2: pH 2 / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; acetic acid; dicyclohexyl-carbodiimide; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2012.04.034

Reference yield:

: 134098-64-9
2‐{3‐[(O‐tert‐butyldimethylsilyl)hydroxy]‐1,1‐dimethylpropyl}‐3,5‐dimethylphenol

: 1381849-05-3
3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0 - 23 °C / Inert atmosphere

2.1: water; acetic acid / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: sodium dihydrogenphosphate; sodium chlorite; water; dihydrogen peroxide / acetonitrile / 0 - 20 °C / Inert atmosphere

4.2: pH 2 / Inert atmosphere

With sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; acetic acid; dicyclohexyl-carbodiimide; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2012.04.034