benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

Base Information

Chemical Name:benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate
CAS No.:1381849-04-2
Molecular Formula:C₂₄H₂₈O₅
Molecular Weight:396.483
Hs Code.:

Synonyms:benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

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Chemical Property of benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

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Technology Process of benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

There total 2 articles about benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-40-2
succinic acid monobenzyl ester

: 1381849-04-2
benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0 - 23 °C / Inert atmosphere

2.1: water; acetic acid / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

With water; acetic acid; dicyclohexyl-carbodiimide; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2012.04.034

Reference yield:

: 134098-64-9
2‐{3‐[(O‐tert‐butyldimethylsilyl)hydroxy]‐1,1‐dimethylpropyl}‐3,5‐dimethylphenol

: 1381849-04-2
benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0 - 23 °C / Inert atmosphere

2.1: water; acetic acid / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / Inert atmosphere

With water; acetic acid; dicyclohexyl-carbodiimide; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2012.04.034

Reference yield: 97.0%

: 1381849-04-2
benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate

: 1381849-05-3
3-(2-(4-(benzyloxy)-4-oxobutanoyloxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

Guidance literature:: benzyl 3,5-dimethyl-2-(2-methyl-4-oxobutan-2-yl)phenyl succinate; With sodium chlorite; sodium dihydrogenphosphate; water; dihydrogen peroxide; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In water; acetonitrile; pH=2; Inert atmosphere;
DOI:10.1016/j.bmc.2012.04.034