N¹-(1-methylethylidene)-1,2-benzenediamine

Base Information

• Chemical Name: N¹-(1-methylethylidene)-1,2-benzenediamine
• CAS No.: 1314909-00-6
• Molecular Formula: C₉H₁₂N₂
• Molecular Weight: 148.208
• Mol file: 1314909-00-6.mol

Synonyms:N¹-(1-methylethylidene)-1,2-benzenediamine

Chemical Property of N¹-(1-methylethylidene)-1,2-benzenediamine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N¹-(1-methylethylidene)-1,2-benzenediamine

There total 4 articles about N¹-(1-methylethylidene)-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1,2-diamino-benzene (95-54-5) + acetone (67-64-1) → 2,2,4-trimethyl-2,3-dihydro-1H-1,5-benzodiazepine (24107-34-4) + N1-(1-methylethylidene)-1,2-benzenediamine (1314909-00-6)

Guidance literature:

With mesoporous aluminosilicate MCM-41-PS; at 65 ℃; for 6h;

DOI:10.1002/chem.200900492

Reference yield:

1,2-diamino-benzene (95-54-5) + acetone (67-64-1) → N1-(1-methylethylidene)-1,2-benzenediamine (1314909-00-6)

Guidance literature:

With metal-benzenetricarboxylate of MIL-100 (V³⁺); In 1,2-dichloro-ethane; at 50 ℃; for 1h; Reagent/catalyst;

DOI:10.1016/j.jcat.2017.08.009

Reference yield:

1,2-diamino-benzene (95-54-5) + acetone (67-64-1) → N1-(1-methylethylidene)-1,2-benzenediamine (1314909-00-6) + 2-methyl-1,4-dihydroquinoxaline

Guidance literature:

With 4-heptylbenzoic acid; at 65 ℃; for 10h; Catalytic behavior; Sealed tube;

DOI:10.1039/c8dt00394g

upstream raw materials:

1,2-diamino-benzene

acetone