(4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one

Base Information

• Chemical Name: (4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one
• CAS No.: 614763-02-9
• Molecular Formula: C₁₇H₁₅FN₂O
• Molecular Weight: 282.317

Synonyms:(4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one

Chemical Property of (4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one

Chemical Property:

Purity/Quality:

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Technology Process of (4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one

There total 2 articles about (4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C19H19FN2O2 (786707-55-9) → (4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one (614763-02-9)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 65 ℃; for 5h;

DOI:10.1016/j.bmcl.2005.03.027

Reference yield:

C13H16O4 → (4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one (614763-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 41 percent / NaOAc / acetic acid / 24 h / 20 °C

2: 100 percent / aq. HCl / tetrahydrofuran / 5 h / 65 °C

With hydrogenchloride; sodium acetate; In tetrahydrofuran; acetic acid;

DOI:10.1016/j.bmcl.2005.03.027

Reference yield: 100.0%

(4αS)-1-(4-fluorophenyl)-4α-methyl-4,4α,6,7-tetrahydrocyclopenta[f]indazol-5(1H)-one (614763-02-9) + Methyltriphenylphosphonium bromide (1779-49-3) → C18H17N2F (614763-03-0)

Guidance literature:

With potassium hexamethylsilazane; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2007.03.103

upstream raw materials:

C₁₉H₁₉FN₂O₂

Downstream raw materials:

C₁₈H₁₇N₂F

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