C₉H₈ClFN₄O

Base Information

Chemical Name:C₉H₈ClFN₄O
CAS No.:1048966-14-8
Molecular Formula:C₉H₈ClFN₄O
Molecular Weight:242.64
Hs Code.:

C<sub>9</sub>H<sub>8</sub>ClFN<sub>4</sub>O

Synonyms:C₉H₈ClFN₄O

Suppliers and Price of C₉H₈ClFN₄O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₈ClFN₄O

Chemical Property:

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Technology Process of C₉H₈ClFN₄O

There total 4 articles about C₉H₈ClFN₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 100563-49-3
C₉H₆ClFN₄O₃

: 1048966-14-8
C₉H₈ClFN₄O

Guidance literature:: With iron; ammonium chloride; In ethanol; water; Reflux;
DOI:10.3390/molecules15129024

Reference yield:

: 112006-20-9
C₉H₈ClFN₂O₂

: 1048966-14-8
C₉H₈ClFN₄O

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; triethylamine / toluene / Reflux

2: sulfuric acid; nitric acid / 0 - 20 °C

3: iron; ammonium chloride / ethanol; water / Reflux

With sulfuric acid; diphenyl phosphoryl azide; nitric acid; iron; ammonium chloride; triethylamine; In ethanol; water; toluene; 1: Schmidt reaction;
DOI:10.3390/molecules15129024

Reference yield:

: 57946-56-2
2-fluoro-4-chloroaniline

: 1048966-14-8
C₉H₈ClFN₄O

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium nitrite / hydrogenchloride; water / 1.5 h / -9 °C / Inert atmosphere; liquid HCl

1.2: -9 - 20 °C / liquid HCl

1.3: 0.5 h / 20 °C / liquid HCl

2.1: diphenyl phosphoryl azide; triethylamine / toluene / Reflux

3.1: sulfuric acid; nitric acid / 0 - 20 °C

4.1: iron; ammonium chloride / ethanol; water / Reflux

With sulfuric acid; diphenyl phosphoryl azide; nitric acid; iron; ammonium chloride; triethylamine; sodium nitrite; In hydrogenchloride; ethanol; water; toluene; 2.1: Schmidt reaction;
DOI:10.3390/molecules15129024