(1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate

Base Information

Chemical Name:(1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate
CAS No.:1075726-74-7
Molecular Formula:C₂H₂O₄*C₂₃H₃₀N₂O₅
Molecular Weight:504.537
Hs Code.:

Synonyms:(1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate

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Chemical Property of (1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate

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Technology Process of (1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate

There total 1 articles about (1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 144-62-7,97993-78-7
oxalic acid

: 54417-53-7,66820-84-6
(R)-tetrahydropapaverine hydrochloride

: 79-06-1,12624-24-7,25038-45-3,27754-57-0,33338-03-3,39387-77-4,68247-81-4,9082-06-8,79079-15-5
2-propenamide

: 1075726-74-7
(1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate

Guidance literature:: (R)-tetrahydropapaverine hydrochloride; With ammonium hydroxide; In water; toluene; at 25 ℃; for 0.25h; pH=9 - 10;

2-propenamide; With acetic acid; In water; toluene; at 80 ℃; for 5h;

oxalic acid; In ethyl acetate; acetone; at 25 ℃; for 0.25h;

Reference yield:

: 1075726-74-7
(1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate

: 74-88-4
methyl iodide

: (1R-trans)-1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methyl-2-aminocarbonylethyl-isoquinolinium iodide

: 1075726-85-0
(1R-cis)-1-[(3,4-dimethoxyphenyl)methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methyl-2-aminocarbonylethyl-isoquinolinium iodide

Guidance literature:: (1R)-1-[(3,4-dimethoxyphenyl)-methyl]-1,2,3,4-tetrahydro-6,7-dimethoxy-2-aminocarbonylethyl-isoquinoline oxalate; With sodium hydroxide; In dichloromethane; water; at 25 ℃; for 0.25h; pH=9 - 10;

methyl iodide; at 25 ℃;