1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine

Base Information

• Chemical Name: 1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine
• CAS No.: 1033192-21-0
• Molecular Formula: C₂₁H₂₄N₂O
• Molecular Weight: 320.434

Synonyms:1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine

Chemical Property of 1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine

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Technology Process of 1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine

There total 2 articles about 1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine (871976-40-8) + isobutylamine (78-81-9) → 2-(3-chloropropyl)-2-phenyl-2H-1,4-benzoxazin-3(4H)-one (871976-44-2) + 1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine (1033192-21-0)

Guidance literature:

1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine; With zinc(II) chloride; In dichloromethane; at 20 ℃; for 30h;

isobutylamine; In dimethyl sulfoxide; at 100 ℃; for 0.25h; Further stages.;

DOI:10.1134/S1070428007070214

Reference yield: 23.0%

1,1-dichloro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine (871976-38-4) + isobutylamine (78-81-9) → 1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine (1033192-21-0)

Guidance literature:

In dimethyl sulfoxide; at 100 ℃; for 2h;

DOI:10.1134/S1070428007070214

upstream raw materials:

1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

isobutylamine

1,1-dichloro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

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