1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

Base Information

Chemical Name:1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine
CAS No.:871976-40-8
Molecular Formula:C₁₇H₁₅ClFNO
Molecular Weight:303.764
Hs Code.:

Synonyms:1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

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Chemical Property of 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

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Technology Process of 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

There total 1 articles about 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 75-43-4
Dichlorofluoromethane

: 87696-97-7
3,4-dihydro-5-phenyl-2H-1,6-benzoxazocine

: 871976-40-8
1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

Guidance literature:: With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; at 8 - 11 ℃; for 0.666667h;
DOI:10.1039/b512409c

Reference yield: 93.0%

: 871976-40-8
1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

: 871976-44-2
2-(3-chloropropyl)-2-phenyl-2H-1,4-benzoxazin-3(4H)-one

Guidance literature:: With zinc(II) chloride; In dichloromethane; at 20 ℃;
DOI:10.1039/b512409c

Reference yield: 64.0%

: 871976-40-8
1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 871976-44-2
2-(3-chloropropyl)-2-phenyl-2H-1,4-benzoxazin-3(4H)-one

: 1033192-32-3
1-[2-(3,4-dimethoxyphenyl)ethyl]-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzoxazine

Guidance literature:: 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzoxazocine; With zinc(II) chloride; In dichloromethane; at 20 ℃; for 0.5h;

2-(3,4-dimethoxyphenyl)-ethylamine; In dimethyl sulfoxide; at 100 ℃; for 0.25h; Further stages.;
DOI:10.1134/S1070428007070214