benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate

Base Information

Chemical Name:benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate
CAS No.:946583-04-6
Molecular Formula:C₃₀H₃₉FN₂O₃Si
Molecular Weight:522.735
Hs Code.:

Synonyms:benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate

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Technology Process of benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate

There total 1 articles about benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 946583-02-4
N-{4-amino-2-fluoro-6-[2-(tert-butyldimethylsilyloxy)ethyl]phenyl}-N-benzyl-N-methylamine

: 501-53-1,94274-21-2
benzyl chloroformate

: 946583-04-6
benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate

Guidance literature:: With pyridine; In dichloromethane; at 23 ℃; for 1h;

Reference yield:

: 415684-05-8
tert-butyl (2S)-3-chloro-2-hydroxypropylcarbamate

: 946583-04-6
benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate

: tert-butyl ((5S)-3-{4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenyl}-2-oxo-1,3-oxazolidin-5-yl)methylcarbamate

Guidance literature:: tert-butyl (2S)-3-chloro-2-hydroxypropylcarbamate; benzyl 4-[benzyl(methyl)amino]-3-fluoro-5-[2-(tert-butyldimethylsilyloxy)ethyl]phenylcarbamate; With lithium tert-butoxide; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 23 ℃; for 20h;

With water; ammonium chloride; In tetrahydrofuran; N,N-dimethyl-formamide;