Technology Process of Benzyl (2S)-2-amino>propionate Hydrogenmaleate
There total 8 articles about Benzyl (2S)-2-amino>propionate Hydrogenmaleate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 28percent aq. NH3 / 168 h / Ambient temperature
3: CoCl2 / H2O / 72 h / 37 °C / aminoacylase (from Aspergillus oryzae); pH 7
4: SOCl2
5: 43.6 percent / K2CO3 / dimethylsulfoxide / 30 h / Ambient temperature
6: ethyl acetate; diisopropyl ether
With
ammonium hydroxide; thionyl chloride; potassium carbonate;
In
di-isopropyl ether; water; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm00122a003
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 30.1 percent / K2CO3 / dimethylsulfoxide / 30 h / Ambient temperature
2: ethyl acetate; diisopropyl ether
With
potassium carbonate;
In
di-isopropyl ether; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm00122a003
- Guidance literature:
-
Multi-step reaction with 5 steps
2: CoCl2 / H2O / 72 h / 37 °C / aminoacylase (from Aspergillus oryzae); pH 7
3: SOCl2
4: 43.6 percent / K2CO3 / dimethylsulfoxide / 30 h / Ambient temperature
5: ethyl acetate; diisopropyl ether
With
thionyl chloride; potassium carbonate;
In
di-isopropyl ether; water; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm00122a003
