tetrakis(p-chlorophenyl)diazine

Base Information

• Chemical Name: tetrakis(p-chlorophenyl)diazine
• CAS No.: 50482-89-8
• Molecular Formula: C₂₆H₁₆Cl₄N₂
• Molecular Weight: 498.238
• Mol file: 50482-89-8.mol

Synonyms:tetrakis(p-chlorophenyl)diazine

Chemical Property of tetrakis(p-chlorophenyl)diazine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of tetrakis(p-chlorophenyl)diazine

There total 6 articles about tetrakis(p-chlorophenyl)diazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4,4'-dichlorobenzophenone hydrazone (5463-11-6) → tetrakis(p-chlorophenyl)diazine (50482-89-8)

Guidance literature:

In acetonitrile; at 17 ℃; for 0.4h; Pt-anode, LiClO₄ as supporting electrolyte, constant current: 0.5 A, electron release: 0.5 F/mol (total: 7.5 mF), applied potl. vs. SCE: 0.8-2.0 V, divided cell;

DOI:10.1021/jo00166a006

Reference yield: 81.0%

(4aR,6S,7S,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol (4148-58-7) + bis-(4-chlorophenyl)diazomethane (1143-92-6) → tetrakis(p-chlorophenyl)diazine (50482-89-8) + methyl 4,6-O-benzylidene-3-O--α-D-mannopyranoside (82186-05-8)

Guidance literature:

tin(ll) chloride; In 1,2-dimethoxyethane; at 17 ℃; for 48h;

DOI:10.1016/S0008-6215(82)80006-2

Reference yield: 80.0%

bis-(4-chlorophenyl)diazomethane (1143-92-6) + 1,2:5,6-di-O-isopropylidene-α-D-glucofuranose (582-52-5) → tetrakis(p-chlorophenyl)diazine (50482-89-8) + 3-O--1,2:5,6-di-O-isopropylidene-α-D-glucofuranose (82185-97-5)

Guidance literature:

In benzene; for 24h; Heating;

DOI:10.1016/S0008-6215(82)80006-2

upstream raw materials:

4,4'-dichlorobenzophenone hydrazone

(4aR,6S,7S,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

bis-(4-chlorophenyl)diazomethane

cis-1,4-anhydroerythritol