(3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

Base Information

Chemical Name:(3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate
CAS No.:1002123-62-7
Molecular Formula:C₁₃H₁₅IO₅S
Molecular Weight:410.23
Hs Code.:

Synonyms:(3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

Suppliers and Price of (3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

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Technology Process of (3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

There total 1 articles about (3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 54522-28-0,66966-12-9,67890-26-0,76793-35-6,107740-09-0
(3R,3aS,6R,6aS)-hexahydrofuro[3,2-b]furan-3,6-diyl bis(4-methylbenzenesulfonate)

: 1002123-62-7
(3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

: 3770-77-2,67890-24-8,128162-60-7
(1R,4R,5R,8S)-(+)-4,8-Diiodo-2,6-dioxabicyclo<3.3.0>octane

: 3770-77-2
(1R,4S,5R,8S)-(+)-4,8-Diiodo-2,6-dioxabicyclo<3.3.0>octane

Guidance literature:: With sodium iodide; In N,N-dimethyl-formamide; at 100 - 135 ℃; for 23h;

Reference yield: 95.0%

: 1002123-62-7
(3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

: 75-36-5
acetyl chloride

: 1007402-49-4
(R)-2-[(S)-2,5-dihydrofuran-2-yl]-2-(tosyloxy)ethyl acetate

Guidance literature:: (3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -75 ℃; for 0.5h;

acetyl chloride; In tetrahydrofuran; hexane; at -75 - 20 ℃; Further stages.;
DOI:10.1016/j.tetasy.2007.11.034

Reference yield: 93.0%

: 1002123-62-7
(3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

: 1001547-70-1
(R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate

Guidance literature:: (3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate; With methyllithium lithium chloride complex; In tetrahydrofuran; diethyl ether; at -70 ℃; for 1.03333h;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; Product distribution / selectivity;