(R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate

Base Information

Chemical Name:(R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate
CAS No.:1001547-70-1
Molecular Formula:C₁₃H₁₆O₅S
Molecular Weight:284.333
Hs Code.:

Synonyms:(R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate

Chemical Property:

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Technology Process of (R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate

There total 6 articles about (R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1002123-62-7
(3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate

: 1001547-70-1
(R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate

Guidance literature:: (3R,3aS,6aS)-6-iodohexahydrofuro[3,2-b]furan-3-yl 4-methylbenzenesulphonate; With methyllithium lithium chloride complex; In tetrahydrofuran; diethyl ether; at -70 ℃; for 1.03333h;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; Product distribution / selectivity;

Reference yield: 75.0%

: (3R,3aS,6S,6aS)-6-bromohexahydrofuro[3,2-b]-3-yl 4-methylbenzenesulfonate

: 1001547-70-1
(R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate

Guidance literature:: With ammonium chloride; zinc; In tetrahydrofuran; water; isopropyl alcohol; at 20 ℃; for 16h; Product distribution / selectivity;

Reference yield:

: (3R,6R)-hexahydrofuro[3,2-b]furan-3,6-diol

: 1001547-70-1
(R)-1-((S)-2,5-dihydrofuran-2-yl)-2-hydroxyethyl 4-methyl-benzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / tetrachloromethane; dichloromethane; water / 26 h / 0 °C / Inert atmosphere

2: pyridine; carbon tetrabromide; triphenylphosphine / N,N-dimethyl-formamide / 65 °C / Inert atmosphere

3: water; ammonium chloride; zinc / tetrahydrofuran; isopropyl alcohol / 16 h / Inert atmosphere

With pyridine; carbon tetrabromide; water; ammonium chloride; triphenylphosphine; potassium hydroxide; zinc; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;