(Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate

Base Information

• Chemical Name: (Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate
• CAS No.: 1393367-72-0
• Molecular Formula: C₁₉H₂₄F₃O₄PS
• Molecular Weight: 436.432

Synonyms:(Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate

Chemical Property of (Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

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Technology Process of (Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate

There total 1 articles about (Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-phenylbistrifluoromethane-sulfonimide (37595-74-7) + 5-hydroxy-1-menthyl-1H-phosphindole 1-oxide → (Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate (1393367-72-0) + (Sp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate (1393367-80-0)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; Inert atmosphere;

DOI:10.1002/anie.201202024

Reference yield: 75.0%

(Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate (1393367-72-0) + (E)-11-(5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)oct-4-en-4-yl)naphtho[1,2-f]quinoline (1449060-42-7) → C43H48NOP (1449060-44-9)

Guidance literature:

With PdCl₂(2-dicyclohexylphosphino-2',6'-dimethoxybiphenyl)2; caesium carbonate; In tetrahydrofuran; water; at 85 ℃; for 18h; Inert atmosphere;

DOI:10.1002/chem.201300844

Reference yield: 74.0%

(Rp)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1-oxo-1H-phosphindol-5-yl trifluoromethanesulfonate (1393367-72-0) + (E)-2-(5-(benzo[c]phenanthren-2-yl)oct-4-en-4-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (1393367-71-9) → (Rp)-5-((Z)-5-(benzo[c]phenanthren-2-yl)oct-4-en-4-yl)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1H-phosphindole 1-oxide (1393367-73-1)

Guidance literature:

With PdCl₂(SPhos)2; caesium carbonate; In tetrahydrofuran; water; at 85 ℃; for 18h;

DOI:10.1002/anie.201202024

upstream raw materials:

N,N-phenylbistrifluoromethane-sulfonimide

Downstream raw materials:

(Rp)-5-((Z)-5-(benzo[c]phenanthren-2-yl)oct-4-en-4-yl)-1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-1H-phosphindole 1-oxide

C₄₃H₄₈NOP

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