phenylethynyl menthyl ether

Base Information

• Chemical Name: phenylethynyl menthyl ether
• CAS No.: 108167-60-8
• Molecular Formula: C₁₈H₂₄O
• Molecular Weight: 256.388
• Mol file: 108167-60-8.mol

Synonyms:phenylethynyl menthyl ether

Chemical Property of phenylethynyl menthyl ether

Chemical Property:

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Technology Process of phenylethynyl menthyl ether

There total 2 articles about phenylethynyl menthyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C19H25F3O4S (1073822-62-4) → phenylethynyl menthyl ether (108167-60-8)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

DOI:10.1021/ol802147h

Reference yield:

triphenylborane (960-71-4) + ethynyl, [2-isopropyl-5-methylcyclohexyl(1R,2S,5R)]ether (108167-50-6) → phenylethynyl menthyl ether (108167-60-8)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, from -25 deg C to 0 deg C, 2.) THF, hexane, 0 deg C 30 min;

DOI:10.1021/jo00389a048

upstream raw materials:

triphenylborane

ethynyl, [2-isopropyl-5-methylcyclohexyl(1R,2S,5R)]ether

C₁₉H₂₅F₃O₄S