N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide

Base Information

Chemical Name:N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide
CAS No.:1383129-55-2
Molecular Formula:C₂₄H₂₉NO₄
Molecular Weight:395.499
Hs Code.:

Synonyms:N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide

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Chemical Property of N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide

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Technology Process of N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide

There total 3 articles about N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1383129-32-5
N-(2,2-diethoxyethyl)-4-methoxy-3,5-dimethylaniline

: 637-44-5
phenylpropyolic acid

: 1383129-55-2
N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c2cc32783j

Reference yield:

: 645-36-3
2,2-diethoxy-ethanamine

: 1383129-55-2
N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / 40 h / 80 °C / Inert atmosphere

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; copper(l) iodide; potassium carbonate; dicyclohexyl-carbodiimide; L-proline; In dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c2cc32783j

Reference yield:

: 55215-54-8
5-iodo-2-methoxy-1,3-dimethylbenzene

: 1383129-55-2
N-(2,2-diethoxyethyl)-N-(4-methoxy-3,5-dimethylphenyl)-3-phenylpropiolamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / 40 h / 80 °C / Inert atmosphere

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; copper(l) iodide; potassium carbonate; dicyclohexyl-carbodiimide; L-proline; In dichloromethane; dimethyl sulfoxide;
DOI:10.1039/c2cc32783j