[Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

Base Information

Chemical Name:[Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)
CAS No.:399039-59-9
Molecular Formula:C₃₀H₃₁OP₂Pd*F₆P
Molecular Weight:720.907
Hs Code.:

[Pd(CH<sub>2</sub>CH<sub>2</sub>CO(CH<sub>3</sub>)(1,2-bis(diphenylphosphino)ethane)](PF<sub>6</sub>)

Synonyms:[Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

Suppliers and Price of [Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

There total 2 articles about [Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 74-85-1
ethene

: 399039-62-4
[Pd(CO)(COCH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

: 399039-59-9
[Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

Guidance literature:: With CD₃CN; In dichloromethane-d2; byproducts: CO; using Schlenk techniques; immersing in bath of soln. of (Pd(CO)(COMe)(dppe))PF6 in CD2Cl2 at -30°C; addn. of CD3CN, purging with Ar; treatment with C2H4 (15 bar) at -110°C;
DOI:10.1021/om010727b

Reference yield:

: 399039-50-0
[Pd(CH₃CN)(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

: 74-85-1
ethene

: 201230-82-2
carbon monoxide

: 399039-59-9
[Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

Guidance literature:: With CH₃CN; In dichloromethane-d2; (N2); using Schlenk techniques; transferring of soln. of PdC29H30F6NP3 in CD2Cl2 into NMR tube, pressing to 15 bar with CO at room temp.; immersing into bath at -40°C; addn. of MeCN at ambient pressure; bubbling of C2H4 for 2 min at -40°C;; transferring from NMR tube into flask immersed in a bath at -20°C, evapn. of solvent under reduced pressure, washing with n-pentane, drying, elem. anal.;
DOI:10.1021/om010727b

Reference yield:

: 399039-59-9
[Pd(CH₂CH₂CO(CH₃)(1,2-bis(diphenylphosphino)ethane)](PF₆)

: 7440-05-3
palladium

Guidance literature:: In dichloromethane-d2; byproducts: methyl ethyl ketone, methyl vinyl ketone; (N2); using Schlenk techniques, charging of NMR tube with soln. of C30H31F6OP3Pd in CD2Cl2 at 20°C, holding at room temp. for 15 h; monitoring by NMR;
DOI:10.1021/om010727b