4b,5a-dihydrodibenzo[c,h]oxireno[a]acridine

Base Information

Chemical Name:4b,5a-dihydrodibenzo[c,h]oxireno[a]acridine
CAS No.:67977-00-8
Molecular Formula:C21H13NO
Molecular Weight:295.334
Hs Code.:

Synonyms:

Suppliers and Price of 4b,5a-dihydrodibenzo[c,h]oxireno[a]acridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 4b,5a-dihydrodibenzo[c,h]oxireno[a]acridine

Chemical Property:

Vapor Pressure:1.72E-11mmHg at 25°C
Boiling Point:547.7°C at 760 mmHg
Flash Point:192.2°C
Density:1.358g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 4b,5a-dihydrodibenzo[c,h]oxireno[a]acridine

There total 10 articles about 4b,5a-dihydrodibenzo[c,h]oxireno[a]acridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 224-53-3
dibenz[c,h]acridine

: 67977-00-8
4b,5a-dihydrodibenzoxireno acridine

Guidance literature:: With sodium hypochlorite; disodium hydrogenphosphate; tetra(n-butyl)ammonium hydrogensulfate; In chloroform; for 5h; Ambient temperature;

Reference yield:

: 90-15-3
α-naphthol

: 67977-00-8
4b,5a-dihydrodibenzoxireno acridine

Guidance literature:: Multi-step reaction with 3 steps

1: 12.9 percent / 0.25 h / 250 °C

2: 10percent Pd/C / 3 h / 330 - 350 °C

3: 10 percent / aq. NaOCl / tetrabutylammonium hydrogen sulfate / CHCl₃ / 5 h / Ambient temperature

With sodium hypochlorite; palladium on activated charcoal; tetra(n-butyl)ammonium hydrogensulfate; In chloroform;
DOI:10.1021/jo00201a019

Reference yield:

: 2217-41-6
1-amino-5,6,7,8-tetrahydronaphthalene

: 67977-00-8
4b,5a-dihydrodibenzoxireno acridine

Guidance literature:: Multi-step reaction with 3 steps

1: 12.9 percent / 0.25 h / 250 °C

2: 10percent Pd/C / 3 h / 330 - 350 °C

3: 10 percent / aq. NaOCl / tetrabutylammonium hydrogen sulfate / CHCl₃ / 5 h / Ambient temperature

With sodium hypochlorite; palladium on activated charcoal; tetra(n-butyl)ammonium hydrogensulfate; In chloroform;
DOI:10.1021/jo00201a019