(S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine

Base Information

Chemical Name:(S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine
CAS No.:1365547-75-6
Molecular Formula:C₁₁H₁₄ClNOS
Molecular Weight:243.757
Hs Code.:

(S<sub>S</sub>)-α-chloro-N-p-toluenesulfinyl isobutyraldimine

Synonyms:(S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine

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Technology Process of (S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine

There total 1 articles about (S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 917-93-1
2-chloroisobutyraldehyde

: 188447-91-8
(S)-p-toluenesulfinimide

: 1365547-75-6
(S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine

Guidance literature:: With titanium(IV) tetraethanolate; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c2ob06637h

Reference yield: 88.0%

: 69555-14-2
ethyl N-diphenylmethylene glycine

: 1365547-75-6
(S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine

: 1365548-17-9
(S(S),2R,3R)-ethyl 2-(diphenylmethyleneamino)-4-chloro-4-methyl-3-(p-toluenesulfinylamino)pentanoate

Guidance literature:: ethyl N-diphenylmethylene glycine; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

(S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/c2ob06637h

Reference yield: 86.0%

: 1365547-75-6
(S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine

: 81167-39-7
methyl N-(diphenylmethylene)glycinate

: 1365548-20-4
(S(S),2R,3R)-methyl 2-(diphenylmethyleneamino)-4-chloro-4-methyl-3-(p-toluenesulfinylamino)pentanoate

Guidance literature:: methyl N-(diphenylmethylene)glycinate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

(S_S)-α-chloro-N-p-toluenesulfinyl isobutyraldimine; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1039/c2ob06637h