(Z)-3-ethoxy-2-iodopropenyl phenyl selenide

Base Information

• Chemical Name: (Z)-3-ethoxy-2-iodopropenyl phenyl selenide
• CAS No.: 863494-73-9
• Molecular Formula: C₁₁H₁₃IOSe
• Molecular Weight: 367.088
• Mol file: 863494-73-9.mol

Synonyms:(Z)-3-ethoxy-2-iodopropenyl phenyl selenide

Chemical Property of (Z)-3-ethoxy-2-iodopropenyl phenyl selenide

Chemical Property:

Purity/Quality:

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Technology Process of (Z)-3-ethoxy-2-iodopropenyl phenyl selenide

There total 1 articles about (Z)-3-ethoxy-2-iodopropenyl phenyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

ethanol (64-17-5) + 1,2-propadienyl phenyl selenide (1595-42-2) → (Z)-3-ethoxy-2-iodopropenyl phenyl selenide (863494-73-9)

Guidance literature:

With iodine; In acetonitrile; at 20 ℃; for 1h;

DOI:10.1016/j.tet.2005.05.077

Reference yield: 79.0%

(Z)-3-ethoxy-2-iodopropenyl phenyl selenide (863494-73-9) + phenylboronic acid (98-80-6) → (E)-3-ethoxy-2-phenylpropenyl phenyl selenide

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In methanol; toluene; for 22.5h; Heating;

DOI:10.1016/j.tet.2005.05.077

Reference yield: 76.0%

(Z)-3-ethoxy-2-iodopropenyl phenyl selenide (863494-73-9) + 4-methoxyphenylboronic acid (5720-07-0) → (E)-3-ethoxy-2-(4'-methoxyphenyl)propenyl phenyl selenide

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In methanol; toluene; for 17.5h; Heating;

DOI:10.1016/j.tet.2005.05.077

upstream raw materials:

ethanol

1,2-propadienyl phenyl selenide