2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime

Base Information

Chemical Name:2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime
CAS No.:1313438-35-5
Molecular Formula:C₂₆H₂₇N₃O
Molecular Weight:397.52
Hs Code.:

Synonyms:2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime

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Chemical Property of 2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime

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Technology Process of 2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime

There total 4 articles about 2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1313439-88-1
tert-butyl (1-(4-(5-(methoxyimino)-3-phenyl-5,6,7,8-tetrahydroquinolin-2-yl)phenyl)cyclobutyl)carbamate

: 1313438-35-5
2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime

Guidance literature:: With trifluoroacetic acid; for 0.00833333h;

Reference yield:

: 1032349-98-6
tert-butyl 1-(4-(2-phenylacetyl)phenyl)cyclobutylcarbamate

: 1313438-35-5
2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime

Guidance literature:: Multi-step reaction with 4 steps

1: 18 h / 80 °C / Inert atmosphere

2: acetic acid / 2 h / 100 °C / Inert atmosphere; Molecular sieve

3: pyridine / ethanol / 90 °C / Inert atmosphere

4: trifluoroacetic acid / 0.01 h

With pyridine; acetic acid; trifluoroacetic acid; In ethanol;

Reference yield:

: 1247897-74-0
tert-butyl (1-(4-(3-(dimethylamino)-2-phenylacryloyl)phenyl)cyclobutyl)carbamate

: 1313438-35-5
2-(4-(1-aminocyclobutyl)phenyl)-3-phenyl-7,8-dihydroquinolin-5(6H)-one O-methyloxime

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 2 h / 100 °C / Inert atmosphere; Molecular sieve

2: pyridine / ethanol / 90 °C / Inert atmosphere

3: trifluoroacetic acid / 0.01 h

With pyridine; acetic acid; trifluoroacetic acid; In ethanol;