(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

Base Information

Chemical Name:(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride
CAS No.:956468-02-3
Molecular Formula:C₁₄H₂₂N₂O₄S*ClH
Molecular Weight:350.867
Hs Code.:

Synonyms:(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

Suppliers and Price of (2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of (2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

There total 4 articles about (2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 956468-01-2
(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-4-(phenylmethyl)piperazine

: 956468-02-3
(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

Guidance literature:: With hydrogenchloride; water; hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃;

Reference yield:

: 956467-99-5
(3S,6S)-4-benzyl-3,6-dimethylpiperazine-2,5-dione

: 956468-02-3
(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: borane-THF / tetrahydrofuran / 7 h / Heating / reflux

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3: hydrogenchloride; water; hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

With hydrogenchloride; borane-THF; water; hydrogen; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 956467-98-4
methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

: 956468-02-3
(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

2: borane-THF / tetrahydrofuran / 7 h / Heating / reflux

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

4: hydrogenchloride; water; hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

With hydrogenchloride; borane-THF; water; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;