4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate

Base Information

Chemical Name:4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate
CAS No.:956467-49-5
Molecular Formula:C₂₂H₃₀N₂O₆S
Molecular Weight:450.556
Hs Code.:

Synonyms:4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate

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Chemical Property of 4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate

Chemical Property:

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Technology Process of 4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate

There total 5 articles about 4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-(chlorosulfonyl)-2-(methyloxy)phenyl methanesulfonate

: 956468-02-3
(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine hydrochloride

: 956467-49-5
4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 72h;

Reference yield:

: 956467-98-4
methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

: 956467-49-5
4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

2: borane-THF / tetrahydrofuran / 7 h / Heating / reflux

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

4: hydrogenchloride; water; hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 72 h / 20 °C

With hydrogenchloride; borane-THF; water; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 956467-99-5
(3S,6S)-4-benzyl-3,6-dimethylpiperazine-2,5-dione

: 956467-49-5
4-[((2S,5S)-4-{[3,4-bis(methyloxy)phenyl]sulfonyl}-2,5-dimethyl-1-piperazinyl)sulfonyl]-2-(methyloxy)phenyl methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: borane-THF / tetrahydrofuran / 7 h / Heating / reflux

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3: hydrogenchloride; water; hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 72 h / 20 °C

With hydrogenchloride; borane-THF; water; hydrogen; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;