C₃₂H₂₇FN₂O₆S₂

Base Information

Chemical Name:C₃₂H₂₇FN₂O₆S₂
CAS No.:1333243-79-0
Molecular Formula:C₃₂H₂₇FN₂O₆S₂
Molecular Weight:618.707
Hs Code.:

C<sub>32</sub>H<sub>27</sub>FN<sub>2</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₃₂H₂₇FN₂O₆S₂

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Chemical Property of C₃₂H₂₇FN₂O₆S₂

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Technology Process of C₃₂H₂₇FN₂O₆S₂

There total 17 articles about C₃₂H₂₇FN₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1333243-78-9
C₃₂H₂₅FN₂O₆S₂

: 1333243-79-0
C₃₂H₂₇FN₂O₆S₂

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 24h; under 2068.65 Torr;

Reference yield:

: 220801-66-1
5-bromo-2-hydroxylphenylacetic acid methyl ester

: 1333243-79-0
C₃₂H₂₇FN₂O₆S₂

Guidance literature:: Multi-step reaction with 16 steps

1.1: 1H-imidazole / dichloromethane / 15 h / 0 - 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

2.2: 1 h / -78 - 0 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

4.1: hydrogenchloride / water; acetone / 1 h / Reflux

5.1: nitric acid / chloroform / 4 h / 20 °C

6.1: ammonium chloride; iron / water; tetrahydrofuran; methanol / 3 h / Reflux

7.1: pyridine / dichloromethane / 15 h / 0 - 20 °C

8.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 15 h / Inert atmosphere; Reflux

9.1: water; lithium hydroxide monohydrate / 1,4-dioxane / 3 h / Reflux

9.2: pH 3

10.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C

10.2: 15 h

11.1: potassium phosphate / [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / N,N-dimethyl-formamide / 15 h / 90 °C / Inert atmosphere

12.1: hydrogen / palladium on activated charcoal / methanol / 24 h / 25 °C / 2068.65 Torr

13.1: iodine; isopentyl nitrite / copper(l) iodide / acetonitrile / 7 h / 25 - 90 °C

14.1: potassium phosphate / [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / N,N-dimethyl-formamide / 15 h / 90 °C / Inert atmosphere

15.1: dihydrogen peroxide / acetic acid / 3 h / 65 °C

16.1: hydrogen / palladium on activated charcoal / methanol / 24 h / 20 °C / 2068.65 Torr

With pyridine; 1H-imidazole; hydrogenchloride; potassium phosphate; lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; water; hydrogen; dihydrogen peroxide; iodine; nitric acid; iron; potassium carbonate; ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; lithium diisopropyl amide; isopentyl nitrite; copper(l) iodide; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; water; acetic acid; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 614-75-5
2-Hydroxyphenylacetic acid

: 1333243-79-0
C₃₂H₂₇FN₂O₆S₂

Guidance literature:: Multi-step reaction with 17 steps

1.1: tetra-N-butylammonium tribromide / 18 h / 20 °C

2.1: 1H-imidazole / dichloromethane / 15 h / 0 - 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

3.2: 1 h / -78 - 0 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

5.1: hydrogenchloride / water; acetone / 1 h / Reflux

6.1: nitric acid / chloroform / 4 h / 20 °C

7.1: ammonium chloride; iron / water; tetrahydrofuran; methanol / 3 h / Reflux

8.1: pyridine / dichloromethane / 15 h / 0 - 20 °C

9.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 15 h / Inert atmosphere; Reflux

10.1: water; lithium hydroxide monohydrate / 1,4-dioxane / 3 h / Reflux

10.2: pH 3

11.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C

11.2: 15 h

12.1: potassium phosphate / [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / N,N-dimethyl-formamide / 15 h / 90 °C / Inert atmosphere

13.1: hydrogen / palladium on activated charcoal / methanol / 24 h / 25 °C / 2068.65 Torr

14.1: iodine; isopentyl nitrite / copper(l) iodide / acetonitrile / 7 h / 25 - 90 °C

15.1: potassium phosphate / [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / N,N-dimethyl-formamide / 15 h / 90 °C / Inert atmosphere

16.1: dihydrogen peroxide / acetic acid / 3 h / 65 °C

17.1: hydrogen / palladium on activated charcoal / methanol / 24 h / 20 °C / 2068.65 Torr

With pyridine; 1H-imidazole; hydrogenchloride; potassium phosphate; lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; water; hydrogen; dihydrogen peroxide; iodine; nitric acid; tetra-N-butylammonium tribromide; iron; potassium carbonate; ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; lithium diisopropyl amide; isopentyl nitrite; copper(l) iodide; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; chloroform; water; acetic acid; N,N-dimethyl-formamide; acetone; acetonitrile;