α-benzyloxy-γ-ketoaldehyde

Base Information

Chemical Name:α-benzyloxy-γ-ketoaldehyde
CAS No.:1051398-24-3
Molecular Formula:C₁₂H₁₄O₃
Molecular Weight:206.241
Hs Code.:

Synonyms:α-benzyloxy-γ-ketoaldehyde

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Chemical Property of α-benzyloxy-γ-ketoaldehyde

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Technology Process of α-benzyloxy-γ-ketoaldehyde

There total 1 articles about α-benzyloxy-γ-ketoaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1051398-30-1
C₁₂H₁₈O₃

: 1051398-24-3
α-benzyloxy-γ-ketoaldehyde

Guidance literature:: C₁₂H₁₈O₃; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.25h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.200800235 DOI:10.1021/jo801604k

Reference yield: 29.0%

: 1051398-24-3
α-benzyloxy-γ-ketoaldehyde

: 2-(1-triisopropylsilanyloxy-vinylsulfanyl)-pyridine

: 35942-94-0
2-(5-methylfuran-2-yl)ethanol

: 1092680-68-6
C₁₄H₂₀O₃

: C₁₄H₂₀O₃

Guidance literature:: 2-(1-triisopropylsilanyloxy-vinylsulfanyl)-pyridine; With zinc(II) chloride; In dichloromethane; at 23 ℃; for 4h; Inert atmosphere;

α-benzyloxy-γ-ketoaldehyde; With triethylsilane; In dichloromethane; at 0 ℃; for 12h; Inert atmosphere;

With diisobutylaluminium hydride; In dichloromethane; at -78 - 0 ℃; for 6h; Inert atmosphere;
DOI:10.1021/jo801604k

Reference yield: 26.0%

: 1051398-24-3
α-benzyloxy-γ-ketoaldehyde

: 199989-16-7
C₁₇H₂₉NOSSi

: 762-72-1
allyl-trimethyl-silane

: 1051398-33-4
C₈H₁₂O₂

: C₁₈H₂₆O₃

Guidance literature:: C₁₇H₂₉NOSSi; With zinc(II) chloride; at 23 ℃; for 4h; Inert atmosphere;

α-benzyloxy-γ-ketoaldehyde; allyl-trimethyl-silane; at 0 ℃; for 12h; Inert atmosphere;

With diisobutylaluminium hydride; at -78 - 0 ℃; for 6h; Inert atmosphere;
DOI:10.1021/jo801604k