Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester

Base Information

Chemical Name:Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester
CAS No.:202270-98-2
Molecular Formula:C₇₆H₈₇O₂₀P₃
Molecular Weight:1413.44
Hs Code.:

Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester

Synonyms:Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester

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Chemical Property of Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester

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Technology Process of Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester

There total 7 articles about Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 202270-97-1
((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

: 107-92-6
butyric acid

: 202270-98-2
Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1021/jo972046p

Reference yield:

: 173672-85-0
D-3-O-benzyl-2,6-di-O-benzyloxymethyl-4,5-di-O-methoxybenzyl-myo-inositol

: 202270-98-2
Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: N,N-isopropylethylammonium 1H-tetrazole / CH₂Cl₂ / 48 h / Ambient temperature

2: H₂O, 1H-tetrazole / CH₂Cl₂ / 1 h / Ambient temperature

3: 96 percent / NaH / dimethylformamide / 0.5 h / Ambient temperature

4: 93 percent / DDQ / CH₂Cl₂; H₂O / 2 h / Ambient temperature

5: 1.) 1H-tetrazole, 2.) m-CPBA / 1.) CH₂Cl₂, room temperature, 1 h, 2.) 30 min

6: p-TsOH*H₂O / methanol / 1 h / Ambient temperature

7: 92 percent / DCC, DMAP / CH₂Cl₂ / Ambient temperature

With 1H-tetrazole; dmap; N,N-isopropylethylamino 1H-tetrazole; water; sodium hydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo972046p

Reference yield:

: 202270-95-9
[2-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-ethyl]-phosphonic acid benzyl ester (1S,2R,3R,4S,5S,6R)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-dihydroxy-cyclohexyl ester

: 202270-98-2
Butyric acid (S)-3-{benzyloxy-[(1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyloxy]-phosphoryl}-1-butyryloxymethyl-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1H-tetrazole, 2.) m-CPBA / 1.) CH₂Cl₂, room temperature, 1 h, 2.) 30 min

2: p-TsOH*H₂O / methanol / 1 h / Ambient temperature

3: 92 percent / DCC, DMAP / CH₂Cl₂ / Ambient temperature

With 1H-tetrazole; dmap; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/jo972046p