((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Base Information

Chemical Name:((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester
CAS No.:202270-97-1
Molecular Formula:C₆₈H₇₅O₁₈P₃
Molecular Weight:1273.25
Hs Code.:

((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Synonyms:((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

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Chemical Property of ((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

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Technology Process of ((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

There total 6 articles about ((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 202270-96-0
[2-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-ethyl]-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

: 202270-97-1
((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Guidance literature:: With toluene-4-sulfonic acid; In methanol; for 1h; Yield given; Ambient temperature;
DOI:10.1021/jo972046p

Reference yield:

: 173672-85-0
D-3-O-benzyl-2,6-di-O-benzyloxymethyl-4,5-di-O-methoxybenzyl-myo-inositol

: 202270-97-1
((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: N,N-isopropylethylammonium 1H-tetrazole / CH₂Cl₂ / 48 h / Ambient temperature

2: H₂O, 1H-tetrazole / CH₂Cl₂ / 1 h / Ambient temperature

3: 96 percent / NaH / dimethylformamide / 0.5 h / Ambient temperature

4: 93 percent / DDQ / CH₂Cl₂; H₂O / 2 h / Ambient temperature

5: 1.) 1H-tetrazole, 2.) m-CPBA / 1.) CH₂Cl₂, room temperature, 1 h, 2.) 30 min

6: p-TsOH*H₂O / methanol / 1 h / Ambient temperature

With 1H-tetrazole; N,N-isopropylethylamino 1H-tetrazole; water; sodium hydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo972046p

Reference yield:

: 202270-95-9
[2-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-ethyl]-phosphonic acid benzyl ester (1S,2R,3R,4S,5S,6R)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-dihydroxy-cyclohexyl ester

: 202270-97-1
((S)-3,4-Dihydroxy-butyl)-phosphonic acid benzyl ester (1R,2R,3S,4R,5R,6S)-3-benzyloxy-2,6-bis-benzyloxymethoxy-4,5-bis-(bis-benzyloxy-phosphoryloxy)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1H-tetrazole, 2.) m-CPBA / 1.) CH₂Cl₂, room temperature, 1 h, 2.) 30 min

2: p-TsOH*H₂O / methanol / 1 h / Ambient temperature

With 1H-tetrazole; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In methanol;
DOI:10.1021/jo972046p