Technology Process of N,N-di(7-bromo-9,9-dihexyl-2-fluorenyl)-N-phenylamine
There total 4 articles about N,N-di(7-bromo-9,9-dihexyl-2-fluorenyl)-N-phenylamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,10-Phenanthroline; copper(l) chloride; potassium hydroxide;
In
toluene;
at 125 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/pola.24604
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutylammomium bromide; sodium hydroxide / tetrahydrofuran; water / 12 h / 80 °C / Inert atmosphere
2: sulfuric acid; iodine; periodic acid / water; acetic acid / 12 h / 80 °C
3: 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide / toluene / 12 h / 125 °C / Inert atmosphere
With
1,10-Phenanthroline; sulfuric acid; tetrabutylammomium bromide; iodine; periodic acid; copper(l) chloride; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; water; acetic acid; toluene;
3: Ullmann coupling;
DOI:10.1002/pola.24604
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutylammomium bromide; sodium hydroxide / tetrahydrofuran; water / 12 h / 80 °C / Inert atmosphere
2: sulfuric acid; iodine; periodic acid / water; acetic acid / 12 h / 80 °C
3: 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide / toluene / 12 h / 125 °C / Inert atmosphere
With
1,10-Phenanthroline; sulfuric acid; tetrabutylammomium bromide; iodine; periodic acid; copper(l) chloride; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; water; acetic acid; toluene;
3: Ullmann coupling;
DOI:10.1002/pola.24604
