7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine

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Chemical Name:7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine
CAS No.:1285536-61-9
Molecular Formula:C₆₂H₇₃Br₂NS
Molecular Weight:1024.14
Hs Code.:

Synonyms:7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine

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Chemical Property of 7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine

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Technology Process of 7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine

There total 6 articles about 7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2026-42-8
diethyl thien-2-ylmethylphosphonate

: 1285536-60-8
4-[bis(2-bromo-9,9-dihexyl-7-fluorenyl)amino]benzaldehyde

: 1285536-61-9
7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; methanol; at 20 ℃; for 12h;
DOI:10.1002/pola.24604

Reference yield:

: 1285536-59-5
N,N-di(7-bromo-9,9-dihexyl-2-fluorenyl)-N-phenylamine

: 1285536-61-9
7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 1,2-dichloro-ethane / 12 h / 0 - 90 °C

2: potassium tert-butylate / tetrahydrofuran; methanol / 12 h / 20 °C

With potassium tert-butylate; trichlorophosphate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; 1: Vilsmeier formylation / 2: Horner-Emmons reaction;
DOI:10.1002/pola.24604

Reference yield:

: 319906-47-3
2-bromo-7-iodo-9,9-bis-n-hexylfluorene

: 1285536-61-9
7-bromo-N-(2-bromo-9,9-dihexyl-7-fluorenyl)-9,9-dihexyl-N-[4-[2-(thio-phen-2-yl)vinyl]phenyl]fluoren-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide / toluene / 12 h / 125 °C / Inert atmosphere

2: trichlorophosphate / 1,2-dichloro-ethane / 12 h / 0 - 90 °C

3: potassium tert-butylate / tetrahydrofuran; methanol / 12 h / 20 °C

With 1,10-Phenanthroline; potassium tert-butylate; copper(l) chloride; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; toluene; 1: Ullmann coupling / 2: Vilsmeier formylation / 3: Horner-Emmons reaction;
DOI:10.1002/pola.24604