ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate

Base Information

Chemical Name:ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate
CAS No.:1290118-44-3
Molecular Formula:C₄₀H₆₄N₄O₁₂
Molecular Weight:792.968
Hs Code.:

Synonyms:ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate

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Chemical Property of ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate

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Technology Process of ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate

There total 4 articles about ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 477260-11-0
tert-butyl-(4-iodophenethyl)carbamate

: 1290118-42-1
tetraethyl 2,2',2'',2'''-(2,2'-(1-ethoxy-1-oxopent-4-en-2-ylazanediyl)bis(ethane-2,1-diyl))bis(azanetriyl)tetraacetate

: 1290118-44-3
ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; PdCl₂(MeCN)₂; In water; N,N-dimethyl-formamide; at 20 - 60 ℃; for 11h;

Reference yield:

: 51992-77-9
pentaethyl diethylenetriamine-N,N,N',N'',N''-pentaacetate

: 1290118-44-3
ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 39 h / 20 - 40 °C

1.2: 70 h / 80 °C

2.1: N-ethyl-N,N-diisopropylamine / PdCl₂(MeCN)₂ / N,N-dimethyl-formamide; water / 11 h / 20 - 60 °C

With N-ethyl-N,N-diisopropylamine; PdCl₂(MeCN)₂; In water; N,N-dimethyl-formamide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1290118-44-3
ethyl (4E)-2-N,N-bis[2-[N',N'-bis[(ethoxycarbonyl)methyl]amino]ethyl]amino-5-(4-[2-[(t-butoxy)carbonylamino]ethyl]phenyl)pento-4-enolate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 1 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / PdCl₂(MeCN)₂ / N,N-dimethyl-formamide; water / 11 h / 20 - 60 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; PdCl₂(MeCN)₂; In tetrahydrofuran; water; N,N-dimethyl-formamide;