5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid

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Chemical Name:5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid
CAS No.:1290118-46-5
Molecular Formula:C₂₅H₃₈N₄O₁₀
Molecular Weight:554.598
Hs Code.:

Synonyms:5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid

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Chemical Property of 5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid

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Technology Process of 5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid

There total 6 articles about 5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1290118-45-4
Ethyl 2-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-5-(4-{2-[(t-butoxy)carbonylamino]ethyl}phenyl)pentanoate

: 1290118-46-5
5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 14h; Reflux;

Reference yield:

: 51992-77-9
pentaethyl diethylenetriamine-N,N,N',N'',N''-pentaacetate

: 1290118-46-5
5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N-dimethyl-formamide / 39 h / 20 - 40 °C

1.2: 70 h / 80 °C

2.1: N-ethyl-N,N-diisopropylamine / PdCl₂(MeCN)₂ / N,N-dimethyl-formamide; water / 11 h / 20 - 60 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 11 h / 20 °C

4.1: hydrogenchloride / water; tetrahydrofuran / 14 h / 20 °C / Reflux

With hydrogenchloride; hydrogen; N-ethyl-N,N-diisopropylamine; PdCl₂(MeCN)₂; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 73918-57-7
p-Iodophenylethylamine

: 1290118-46-5
5-[4-(2-aminoethyl)phenyl]-2-(N,N-bis{2-N',N'-bis[(carboxymethyl)amino]ethyl}amino)pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 1 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / PdCl₂(MeCN)₂ / N,N-dimethyl-formamide; water / 11 h / 20 - 60 °C

3: hydrogen / palladium 10% on activated carbon / ethanol / 11 h / 20 °C

4: hydrogenchloride / water; tetrahydrofuran / 14 h / 20 °C / Reflux

With hydrogenchloride; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; PdCl₂(MeCN)₂; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;