4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one

Base Information

Chemical Name:4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one
CAS No.:168916-93-6
Molecular Formula:C₃₁H₄₄O₃Sn
Molecular Weight:583.399
Hs Code.:

Synonyms:4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one

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Chemical Property of 4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one

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Technology Process of 4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one

There total 1 articles about 4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: [4-(tri-n-butylstannyl)phenyl]lithium

: 114094-71-2
3-isopropoxy-4-phenylcyclobut-3-ene-1,2-dione

: 168916-93-6
4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one

Guidance literature:: With ammonium chloride; In tetrahydrofuran; mixing at -100°C, stirring (-78°C, 1 h), quenching with NH4Cl; chromatographic workup; elem. anal.;
DOI:10.1021/ja00117a009

Reference yield: 84.0%

: 168916-93-6
4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one

: 74-88-4
methyl iodide

: 168917-35-9
4-methoxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)phenyl]-2-cyclobutene

Guidance literature:: With potassium carbonate; silver(l) oxide; In acetonitrile; stirring (room temp., 2 days), filtration, concn. of the filtrate; chromatography; elem. anal.;
DOI:10.1021/ja00117a009

Reference yield: 80.0%

: 168916-93-6
4-hydroxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one

: 168917-01-9
2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)1,4-naphthoquinone

Guidance literature:: With air; In xylene; reflux 1 h, cooling to room temp., evapn. of the solvent, exposition to air (overnight); chromatography; elem. anal.;
DOI:10.1021/ja00117a009