2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether

Base Information

• Chemical Name: 2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether
• CAS No.: 851517-30-1
• Molecular Formula: C₁₄H₂₀O₅
• Molecular Weight: 268.31
• Mol file: 851517-30-1.mol

Synonyms:2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether

Chemical Property of 2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of 2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether

There total 1 articles about 2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-isopropyl-6-formyl-4-methoxycarbonyl-5-methyl resorcinol dimethyl ether → 2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether (851517-30-1)

Guidance literature:

With sulfuric acid; dihydrogen peroxide; In methanol; at 20 ℃; for 10h;

DOI:10.1055/s-2004-837305

Reference yield: 84.0%

2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether (851517-30-1) → 2-isopropyl-4-hydroxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether

Guidance literature:

With potassium hydroxide; In ethylene glycol; at 130 ℃; for 2h;

DOI:10.1055/s-2004-837305

Reference yield:

2-isopropyl-4-methoxycarbonyl-5-methyl-6-hydroxy resorcinol dimethyl ether (851517-30-1) → 2-isopropyl-4-hydroxy-5-methyl resorcinol dimethyl ether (135626-41-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / aq. KOH / ethane-1,2-diol / 2 h / 130 °C

2: 52 percent / quinoline; CuO / 0.25 h / 215 °C

With quinoline; potassium hydroxide; copper(II) oxide; In ethylene glycol;

DOI:10.1055/s-2004-837305

Downstream raw materials:

2-isopropyl-4-hydroxy-5-methyl resorcinol dimethyl ether